Choosing the right strategy: cryogrinding
The grinding was performed in a dry state using a cryogenic grinder 6970EFM Freezer/Mill® (6970 EFM, SPEX SamplePrep, Metuchen, NJ, USA) which consisted of two stainless steel vessels, with each being able to hold four standard grinding vials. The mill was equipped with a totally enclosed liquid nitrogen (LN 2) auto-fill system, …